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Chin. J. Org. Chem. ›› 2007, Vol. 27 ›› Issue (10): 1305-1308. Previous Articles    

Reports

2-薁基取代的苯并[b]呋喃类化合物的合成

王道林*，徐姣，韩珊，谷峥   

  1. (渤海大学化学化工学院 辽宁省应用化学重点实验室 锦州 121003)
  • 收稿日期:2006-10-09 修回日期:2007-03-13 发布日期:2007-09-28
  • 通讯作者: 王道林

Synthesis of 2-Azulen-2'-ylbenzo[b]furan Derivatives

WANG Dao-Lin*,XU Jiao,HAN Shan,GU Zheng   

  1. (Liaoning Key Laboratory of Applied Chemistry, College of Chemistry and Chemical Engineer-ing,
    Bohai University, Jinzhou 121003)
  • Received:2006-10-09 Revised:2007-03-13 Published:2007-09-28
  • Contact: WANG Dao-Lin

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2-Azulen-2'-ylbenzo[b]furans were obtained via coupling reaction of 2-bromomethylazulene with salicylaldehydes under thermal and microwave irradiation conditions. The bromination conditions of 1-cyano-2-methylazulene with N-bromosuccinimide were discussed. All the compounds were fully characterized by 1H NMR, IR spectra and elemental analysis.

Key words: benzo[b]furan, salicylaldehyde, microwave irradiation, synthesis, azulene