Synthesis and Characterization of Aliphatic Diamine Sulphonate

Chin. J. Org. Chem. ›› 2009, Vol. 29 ›› Issue (06): 904-908. Previous Articles Next Articles

Original Articles

乙二胺基乙磺酸钠的合成与表征

康平平^a; 宋文生^*,a ; 韩冰冰^a; 许双双^b

(a河南科技大学化工与制药学院洛阳 471000)
(b中国石油大学(北京)化工学院环境中心北京 102249)

收稿日期:2008-09-27 修回日期:2008-11-28 发布日期:2009-06-20
通讯作者: 宋文生

Synthesis and Characterization of Aliphatic Diamine Sulphonate

Kang, Pingping^a ; Song, Wensheng^*,a ; Han, Bingbing^a ; Xu, Shuangshuang^b

(a Chemical Engineering and Pharmaceutics College, Henan University of Science and Technology, Luoyang 471000)
(b Environmental Center of Faculty of Chemical Engineering, China University of Petroleum, Beijing 102249)

Received:2008-09-27 Revised:2008-11-28 Published:2009-06-20
Contact: Song, Wensheng

Abstract

Aliphatic diamine sulphonate was synthesized by the reaction of ethylenediamine with sodium 2-chloroethanesulfonate. The products were characterized by means of FTIR, 1H NMR, 13C NMR, XRD, and elemental analysis. The content of aliphatic diamine sulphonate in the product was 94.4% when the mo-lar ratio between ethylenediamine and sodium 2-chloroethanesulfonate was 6.5∶1. The product was more soluble in water, slightly soluble in methanol and ethanol, and insoluble in such organic solvent as acetone, DMF, CCl4, and CHCl3.

Key words: sodium 2-chloroethanesulfonate, characterizati, aliphatic diamine sulphonate, synthesis, ethylenediamine

Cite this article

Kang, Pingping^a ; Song, Wensheng^*,a ; Han, Bingbing^a ; Xu, Shuangshuang^b. Synthesis and Characterization of Aliphatic Diamine Sulphonate[J]. Chin. J. Org. Chem., 2009, 29(06): 904-908.

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乙二胺基乙磺酸钠的合成与表征

Synthesis and Characterization of Aliphatic Diamine Sulphonate

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