Synthesis and Fluorescence Spectral Study of Triaryl Pyrazoline Oxadiazole Compounds

Chin. J. Org. Chem. ›› 2010, Vol. 30 ›› Issue (07): 1039-1043. Previous Articles Next Articles

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三芳基吡唑啉噁二唑类衍生物的合成及其荧光光谱研究

刘计福¹，李东风*¹，唐鑫¹，蔡然¹，韩啸¹，谢志元²

(¹长春工业大学化学与生命科学学院长春 130012)
(²长春应用化学研究所高分子物理与化学国家重点实验室长春 130022)

收稿日期:2009-08-19 修回日期:2009-11-18 发布日期:2010-02-23
通讯作者: 李东风 E-mail:dongfli626@sohu.com
基金资助:
国家级.国家自然科学基金

Synthesis and Fluorescence Spectral Study of Triaryl Pyrazoline Oxadiazole Compounds

Liu Jifu¹ Li Dongfeng*¹ Tang Xin¹ Cai Ran¹ Han Xiao¹ Xie Zhiyuan²

(¹School of Chemistry and Life Science, Changchun University of Technology, Changchun 130012) (²State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Changchun 130022)

Received:2009-08-19 Revised:2009-11-18 Published:2010-02-23
Contact: Dong-Feng Li E-mail:dongfli626@sohu.com

Abstract

A new method of synthesizing 1,3,4-oxadiazole compound was described. The synthesized 1,3,4- oxadiazole compounds were connected with 1,3,5-triaryl-2-pyrazoline through Wittig reaction, and six new triaryl pyrazoline oxadiazole compounds were synthesized. Their structures were characterized by IR, MS, H NMR techniques and elemental analysis. The fluorescence properties were measured by fluorometry, and the test results showed that the target compounds have good fluorescence and λ ranged from 437 to 511 nm, fluorescence quantum yield up to 0.36.

Key words: oxadiazole, pyrazoline, fluorescence, synthesis

Cite this article

LIU Ji-Fu, LI Dong-Feng, TANG Xin, CAI Ran, HAN Xiao, XIE Zhi-Yuan. Synthesis and Fluorescence Spectral Study of Triaryl Pyrazoline Oxadiazole Compounds[J]. Chin. J. Org. Chem., 2010, 30(07): 1039-1043.

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三芳基吡唑啉噁二唑类衍生物的合成及其荧光光谱研究

Synthesis and Fluorescence Spectral Study of Triaryl Pyrazoline Oxadiazole Compounds

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