Synthesis of 2,5-dimethyl-4-hydroxy-3(2H) furanone

Chin. J. Org. Chem. ›› 1997, Vol. 17 ›› Issue (5): 454-457. Previous Articles Next Articles

Original Articles

2,5-二甲基-4-羟基-3(2H)呋喃酮的合成

朱洪友;刘复初;林军;汪有初

云南大学化学系;中国科学院昆明植物研究所

发布日期:1997-10-25

Synthesis of 2,5-dimethyl-4-hydroxy-3(2H) furanone

ZHU HONGYOU;LIU FUCHU;LIN JUN;WANG YOUCHU

Published:1997-10-25

Abstract

2,5-Dimethyl-4-hydroxy-3(2H) furanone has been synthesized by the electrolytic oxidative coupling of acetylacetone followed by Paal-Knorr cyclization, Baeyer-Villiger oxidation and hydrolysis processes. Intermediate 4 and by-product 5 are new compounds.

Key words: HYROLYSIS, COUPLED, HETEROCYCLIC COMPOUNDS, ELECTROLYSIS, OXIDATION REACTION, ORGANIC SYNTHESIS, ACETOPREPANONE, RING CLOSURE REACTION, SYNTHETIC PERFUMES, FURANONE P

CLC Number:

O621

Cite this article

ZHU HONGYOU;LIU FUCHU;LIN JUN;WANG YOUCHU. Synthesis of 2,5-dimethyl-4-hydroxy-3(2H) furanone[J]. Chin. J. Org. Chem., 1997, 17(5): 454-457.

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2,5-二甲基-4-羟基-3(2H)呋喃酮的合成

Synthesis of 2,5-dimethyl-4-hydroxy-3(2H) furanone

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