Chin. J. Org. Chem. ›› 2011, Vol. 31 ›› Issue (12): 2167-2172. Previous Articles     Next Articles

Notes

苯磺酰硫脲衍生物的无溶剂合成

骆崇荣,陈楠楠,华德智,杨高升*   

  1. (安徽师范大学化学与材料科学学院 芜湖 241000)
  • 收稿日期:2011-02-21 修回日期:2011-07-07 发布日期:2011-09-02
  • 通讯作者: 杨高升 E-mail:gshyang@mail.ahnu.edu.cn;

Solvent-Free Synthesis of Benzenesulfonylthioureas

LUO Chong-Rong, CHEN Nan-Nan, HUA De-Zhi, YANG Gao-Sheng   

  1. (College of Chemistry and Materials Science, Anhui Normal University, Wuhu 241000)
  • Received:2011-02-21 Revised:2011-07-07 Published:2011-09-02

A series of benzenesulfonylthioureas were synthesized by the reaction of sodium benzenesulfamides and isosulfocyanates in sealed tube at 130 ℃ and solvent-free conditions in moderate to good yields. All products were characterized by IR, 1H NMR, 13C NMR, ESI-MS techniques and elemental analysis.

Key words: sulfonylthiourea, sulfonamide, isosulfocyanate, solvent-free synthesis