Synthesis, Characterization and Crystal Structure of the Compound Derivedfrom 1-Phenyl-3-methyl-4-benzoyl-5-pyrazolone (HPMBP) and  Glycine Methyl Ester

Chinese Journal of Organic Chemistry ›› 2004, Vol. 24 ›› Issue (2): 195-198. Previous Articles Next Articles

1-苯基-3-甲基-4-苯甲酰基-5-吡唑啉酮(HPMBP)缩甘氨酸甲酯的合成、表征和晶体结构

张欣^*, 朱华玲, 徐海珍, 王瑾玲

天津师范大学化学与生命科学学院天津 300074

收稿日期:2003-05-06 修回日期:2003-08-07 接受日期:2003-08-28 发布日期:2022-09-20
基金资助:
天津市高等学校科技发展基金(No. 01-20601)、天津市自然科学基金(No. 023606511)资助项目

Synthesis, Characterization and Crystal Structure of the Compound Derivedfrom 1-Phenyl-3-methyl-4-benzoyl-5-pyrazolone (HPMBP) and Glycine Methyl Ester

ZHANG, Xin^*, ZHU, Hua-Ling, XU, Hai-Zhen, WANG, Jin-Ling

College of Chemistry and Life, Tianjin Normal University, Tianjin 300074

Received:2003-05-06 Revised:2003-08-07 Accepted:2003-08-28 Published:2022-09-20
Contact: * E-mail: zxin_-tj@eyou.com

Abstract

A new compound derived from 1-phenyl-3-methyl-4-benzoyl-5-pyrazolone and glycine methyl ester has been synthesized and characterized by IR, ¹H NMR spectra and elemental analysis. A full X-ray crystal structure analysis of the compound has been performed. The crystal is Triclinic, space group is P1, a=0.9403(3) nm, b=0.9884(3) nm, c=1.0127(3) nm,α=86.666(7)°, β=89.827(6)°, γ=73.951(6)°, V=0.9029(5) nm³, Z=2, D_c=1.285 Mg·m^-3, μ=0.088 mm^-1, F(000)=368. R₁=0.0452, wR₂=0.0889.

Key words: 1-phenyl-3-methyl-4-benzoyl-5-pyrazolone, glycine methyl ester, synthesis, crystal structure

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ZHANG, Xin, ZHU, Hua-Ling, XU, Hai-Zhen, WANG, Jin-Ling. Synthesis, Characterization and Crystal Structure of the Compound Derivedfrom 1-Phenyl-3-methyl-4-benzoyl-5-pyrazolone (HPMBP) and Glycine Methyl Ester[J]. Chinese Journal of Organic Chemistry, 2004, 24(2): 195-198.

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1-苯基-3-甲基-4-苯甲酰基-5-吡唑啉酮(HPMBP)缩甘氨酸甲酯的合成、表征和晶体结构

Synthesis, Characterization and Crystal Structure of the Compound Derivedfrom 1-Phenyl-3-methyl-4-benzoyl-5-pyrazolone (HPMBP) and Glycine Methyl Ester

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