Synthesis of Pentaerythritol Diacetals from Aldehydes and Ketones under Microwave Irradiation

Chinese Journal of Organic Chemistry ›› 2004, Vol. 24 ›› Issue (11): 1485-1488. Previous Articles

微波辐射条件下季戊四醇双缩醛和双缩酮化合物的合成

靳通收^*, 张伏生, 王开芳, 李同双

河北大学化学与环境科学学院保定 071002

收稿日期:2004-04-27 修回日期:2004-06-03 接受日期:2004-06-09 发布日期:2022-09-21
通讯作者: ^* E-mail: orgsyn@mail.hbu.edu.cn; Fax: +86-312-5079525.
基金资助:
国家自然科学基金(No. 29872011)、教育部高等学校青年骨干教师基金和河北省教育厅基金(No. 990104)资助项目.

Synthesis of Pentaerythritol Diacetals from Aldehydes and Ketones under Microwave Irradiation

JIN Tong-Shou^*, ZHANG Fu-Sheng, WANG Kai-Fang, LI Tong-Shuang

College of Chemistry and Environment Science, Hebei University, Baoding 071002

Received:2004-04-27 Revised:2004-06-03 Accepted:2004-06-09 Published:2022-09-21

Abstract

The pentaerythritol diacetals were effectively synthesized through condensation reaction of pentaerythritol with aldehydes and ketones promoted by zirconium sulfate-silica gel under microwave irradiation. The easy procedure provided a neat environment-friendly synthetic method for pentaerythritol diacetals in high yields and the catalyst was reusable.

Key words: microwave, diacetal, pentaerythritol, aldehyde, ketone, synthesis

Cite this article

JIN Tong-Shou, ZHANG Fu-Sheng, WANG Kai-Fang, LI Tong-Shuang. Synthesis of Pentaerythritol Diacetals from Aldehydes and Ketones under Microwave Irradiation[J]. Chinese Journal of Organic Chemistry, 2004, 24(11): 1485-1488.

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微波辐射条件下季戊四醇双缩醛和双缩酮化合物的合成

Synthesis of Pentaerythritol Diacetals from Aldehydes and Ketones under Microwave Irradiation

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