Chin. J. Org. Chem. ›› 1998, Vol. 18 ›› Issue (4): 334-336. Previous Articles     Next Articles

Original Articles

3, 5-二氯苯胺的电化学合成

马淳安;童少平;高晓萍;张文魁;陈骁军;沈明杰   

  1. 浙江工业大学化工学院;浙江省化工研究院
  • 发布日期:1998-08-25

Electrosynthesis of 3, 5-dichloroaniline

MA CHUNAN;TONG SHAOPING;GAO XIAOPING;ZHANG WENKUI;CHEN XIAOJUN;SHEN MINGJIE   

  • Published:1998-08-25

At 65℃ 3, 5-dichloroaniline is produced from 3, 5-dinitrobenzene at a rotating cathode in divided cell in the following conditions: current density 10A/dm^2; rotating speed of cathode 400r/min; cathode potential -0.35V~-0.45V. The yield of 3, 5-dichloroaniline is about 90%, m.p. 49-52℃.

Key words: NITROBENZENE P, DICHLOROBENZENE P, ELECTROCHEMICAL SYNTHESIS, DICHLOROBENZENE P, BENZAMINE P

CLC Number: