Rapid and Efficient Synthesis of Novel Aryloxyacetyl Hydrazone Molecular Tweezers in Solvent-Free Conditions under Microwave Irradiation

Chin. J. Org. Chem. ›› 2010, Vol. 30 ›› Issue (06): 871-876. Previous Articles Next Articles

Reviews

新的芳杂环酰腙分子钳的微波无溶剂快速有效合成

石培育，刘玲玲，李晓蕊，赵志刚*，刘兴利

西南民族大学化学与环境保护学院成都 610041

收稿日期:2009-10-12 修回日期:2009-11-10 发布日期:2010-01-20
通讯作者: 赵志刚 E-mail:zzg63129@yahoo.com.cn

Rapid and Efficient Synthesis of Novel Aryloxyacetyl Hydrazone Molecular Tweezers in Solvent-Free Conditions under Microwave Irradiation

SHI Pei-Yu, LIU Ling-Ling, LI Xiao-Rui, ZHAO Zhi-Gang, LIU Xing-Li

College of Chemistry and Environmental Protection Engineering, Southwest University for Nationalities, Chengdu 610041

Received:2009-10-12 Revised:2009-11-10 Published:2010-01-20
Contact: Zhi-Gang ZHAO E-mail:zzg63129@yahoo.com.cn

Abstract

Twelve new aryloxyacetyl hydrazone molecular tweezers have been designed and synthesized with high yields using solid Al₂O₃ as supporter and resorcinol as the starting material in solvent-free conditions under microwave irradiation. The structures of all molecular tweezers were characterized by ¹H NMR, IR, mass spectra and elemental analysis. Compared with the conventional heating method, this method is simple, fast, efficient and eco-friendly. The recognition properties of these molecular tweezers for aromatic amines were investigated by UV-Vis spectral titration.

Key words: aryloxyacetyl hydrazone, molecular tweezer, microwave irradiation, synthesis

Cite this article

SHI Pei-Yu, LIU Ling-Ling, LI Xiao-Rui, ZHAO Zhi-Gang, LIU Xing-Li. Rapid and Efficient Synthesis of Novel Aryloxyacetyl Hydrazone Molecular Tweezers in Solvent-Free Conditions under Microwave Irradiation[J]. Chin. J. Org. Chem., 2010, 30(06): 871-876.

Export EndNote|Reference Manager|ProCite|BibTeX|RefWorks

[1]	Fakai Zou, Nengzhong Wang, Hui Yao, Hui Wang, Mingguo Liu, Nianyu Huang. Regio- and Stereo-selective Synthesis of 1β-/3R-Aryl Thiosugar [J]. Chinese Journal of Organic Chemistry, 2024, 44(2): 593-604.
[2]	Luyao Li, Zhongwen He, Zhenguo Zhang, Zhenhua Jia, Teck-Peng Loh. Application of Triaryl Carbenium in Organic Synthesis [J]. Chinese Journal of Organic Chemistry, 2024, 44(2): 421-437.
[3]	Qinggang Mei, Qinghan Li. Recent Progress of Visible Light-Induced the Synthesis of C(3) (Hetero)arylthio Indole Compounds [J]. Chinese Journal of Organic Chemistry, 2024, 44(2): 398-408.
[4]	Penghui Li, Qingyang Xie, Fuxian Wan, Yuanhong Zhang, Lin Jiang. Synthesis and Fungicidal Activity of Novel Substituted Pyrimidine-5-carboxamides Bearing Cyclopropyl Moiety [J]. Chinese Journal of Organic Chemistry, 2024, 44(2): 650-656.
[5]	Shihang Yu, Jiawei Liu, Biyu An, Qinghua Bian, Min Wang, Jiangchun Zhong. Asymmetric Synthesis of the Contact Sex Pheromone of Neoclytus acuminatus acuminatus (Fabricius) [J]. Chinese Journal of Organic Chemistry, 2024, 44(1): 301-308.
[6]	Weiqing Yang, Yanbing Ge, Yuanyuan Chen, Ping Liu, Haiyan Fu, Menglin Ma. Design and Synthesis of Fluorescent 1,8-Napthalimide Derivatives and Their Identification of Cysteine [J]. Chinese Journal of Organic Chemistry, 2024, 44(1): 180-194.
[7]	Qianfan Zhao, Yongzheng Chen, Shiming Zhang. Application and Mechanism Study of Carbon-Based Metal-Free Catalysts in Organic Synthesis [J]. Chinese Journal of Organic Chemistry, 2024, 44(1): 137-147.
[8]	Shan Chen, Zhilin Chen, Qiong Hu, Yanshuang Meng, Yue Huang, Pingfang Tao, Liru Lu, Guobao Huang. Recognition of Bis-thiourea Tweezers to Neutral Molecules in Non-Polar Solvent [J]. Chinese Journal of Organic Chemistry, 2024, 44(1): 277-281.
[9]	Huakun Wang, Xiaolong Ren, Yining Xuan. Study of the Halide Salt Catalyzed [3＋2] Cycloaddition of α,β-Epoxy Carboxylate with Isocyanate [J]. Chinese Journal of Organic Chemistry, 2024, 44(1): 251-258.
[10]	Yukun Jin, Baoyi Ren, Fushun Liang. Visible Light-Mediated Selective C—F Bond Cleavage of Trifluoromethyl Groups and Its Application in Synthesizing gem-Difluoro-Containing Compounds [J]. Chinese Journal of Organic Chemistry, 2024, 44(1): 85-110.
[11]	Cuiyun Ma, Hailan Luo, Fuhua Zhang, Dan Guo, Shuxing Chen, Fei Wang. Green Biosynthesis, Photophysical Properties and Application of 3-Pyrrolyl BODIPY [J]. Chinese Journal of Organic Chemistry, 2024, 44(1): 216-223.
[12]	Bozhen Wang, Jie Zhang, Chunhui Nian, Mingming Jin, Miaomiao Kong, Wulan Li, Wenfei He, Jianzhang Wu. Synthesis and Antitumor Activity of 3,4-Dichlorophenyl Amides [J]. Chinese Journal of Organic Chemistry, 2024, 44(1): 232-241.
[13]	Yang Li, Jinding Yuan, Di Zhao. Deep Eutectic Solvent of 1,3-Dimethylurea/L-(+)-Tartaric Acid for the Green Synthesis of (E)-2-Styrylquinoline-3-carboxylic Acid Derivatives [J]. Chinese Journal of Organic Chemistry, 2023, 43(9): 3268-3276.
[14]	Dandan Sui, Nannan Cen, Ruoqu Gong, Yang Chen, Wenbo Chen. Supporting-Electrolyte-Free Electrochemical Synthesis of Trifluoromethylated Oxindoles in Continuous Flow [J]. Chinese Journal of Organic Chemistry, 2023, 43(9): 3239-3245.
[15]	Huanqing Li, Zhaohua Chen, Zujia Chen, Qiwen Qiu, Youcai Zhang, Sihong Chen, Zhaoyang Wang. Research Progress in Mercury Ion Fluorescence Probes Based on Organic Small Molecules [J]. Chinese Journal of Organic Chemistry, 2023, 43(9): 3067-3077.

新的芳杂环酰腙分子钳的微波无溶剂快速有效合成

Rapid and Efficient Synthesis of Novel Aryloxyacetyl Hydrazone Molecular Tweezers in Solvent-Free Conditions under Microwave Irradiation

PDF

Knowledge

Cited

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments