有机太阳能电池热失效机制及三元共混提升其热稳定性研究进展

doi:10.6023/A22110462

化学学报 ›› 2023, Vol. 81 ›› Issue (2): 131-145.DOI: 10.6023/A22110462 上一篇下一篇

综述

有机太阳能电池热失效机制及三元共混提升其热稳定性研究进展

查汉^a^,^b, 房进^b, 闫翎鹏^a^,^c^,^*(), 杨永珍^c^,^d^,^*(), 马昌期^b^,^*()

a 太原理工大学材料科学与工程学院太原 030024
b 中国科学院苏州纳米技术与纳米仿生研究所创新实验室&印刷电子研究中心苏州 215123
c 太原理工大学新材料界面科学与工程教育部重点实验室太原 030024
d 山西浙大新材料与化工研究院太原 030032

投稿日期:2022-11-14 发布日期:2022-12-23
通讯作者: 闫翎鹏, 杨永珍, 马昌期

作者简介:

查汉, 太原理工大学材料科学与工程学院2020级硕士研究生, 现于中科院苏州纳米技术与仿生研究所联合培养, 研究方向为有机太阳能电池的衰减机理和稳定性提升.

闫翎鹏, 太原理工大学副研究员, 工学博士, 硕士研究生导师, 研究方向包括: 有机太阳能电池的衰减机理及其稳定性提升研究, 碳纳米材料制备、功能化及其光电应用.

杨永珍, 太原理工大学教授, 工学博士, 博士研究生导师, 主要从事纳米碳功能材料、碳基光电材料和生物医药材料的研究. 马昌期, 中国科学院苏州纳米技术与纳米仿生研究所研究员, 中国科学院百人计划研究员, 博士生导师, 主要研究方向包括: 有机光电功能半导体材料与器件, 特别是可印刷光电半导体材料以及印刷制备纳米薄膜光电器件工艺与性能研究.

马昌期, 中国科学院苏州纳米技术与纳米仿生研究所研究员, 中国科学院百人计划研究员, 博士生导师, 主要研究方向包括: 有机光电功能半导体材料与器件, 特别是可印刷光电半导体材料以及印刷制备纳米薄膜光电器件工艺与性能研究.

基金资助:
国家自然科学基金(61904121); 国家自然科学基金(22075315); 国家自然科学基金(22109172); 山西浙大新材料与化工研究院科技研发项目(2022SX-TD012); 山西浙大新材料与化工研究院科技研发项目(2021SX-TD012)

Research Progress of Thermal Failure Mechanism and Ternary Blending to Improve Thermal Stability of Organic Solar Cells

Han Zha^a^,^b, Jin Fang^b, Lingpeng Yan^a^,^c(), Yongzhen Yang^c^,^d(), Changqi Ma^b()

a College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China
b i-Lab & Printable Electronics Research Center, Suzhou Institute of Nano-Tech and Nano-Bionics, Chinese Academy of Sciences, Suzhou 215123, China
c Key Laboratory of Interface Science and Engineering in Advanced Materials, Taiyuan University of Technology, Taiyuan 030024, China
d Shanxi-Zheda Institute of Advanced Materials and Chemical Engineering, Taiyuan 030032, China

Received:2022-11-14 Published:2022-12-23
Contact: Lingpeng Yan, Yongzhen Yang, Changqi Ma
Supported by:
National Natural Science Foundation of China(61904121); National Natural Science Foundation of China(22075315); National Natural Science Foundation of China(22109172); Shanxi-Zheda Institute of Advanced Materials and Chemical Engineering(2022SX-TD012); Shanxi-Zheda Institute of Advanced Materials and Chemical Engineering(2021SX-TD012)

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1. Supporting Information-A22110462.pdf(256KB)

摘要/Abstract

有机太阳能电池(Organic solar cells, OSCs)作为一种新兴高效太阳能电池, 近年来得到飞速发展. 目前OSCs的光电转换效率(Power conversion efficiency, PCE)已经达到19%以上, 初见商业化应用曙光. 但其稳定性方面尚未发展成熟, 尤其在制备和工作过程中电池器件需要经历高温考验, 电池的热稳定性要求高. 三元共混策略是在传统的二元OSCs活性层中引入第三组分, 利用第三组分调控分子间的相互作用, 在实现高效光电转换效率的同时有效提高器件热稳定性, 展现出了极大的应用潜力. 本综述首先从器件热衰减过程出发, 总结了OSCs热衰减过程中包括: 热致活性层形貌变化、各层材料之间的互扩散行为以及界面老化等相关机制. 在此基础上, 重点介绍了三元策略在提高OSCs热稳定性方面的应用进展和作用机制. 最后, 对三元策略在OSCs中的应用发展进行总结并展望, 指出第三组分的针对性选择以及作用机制解析是三元OSCs面临的关键问题和挑战.

关键词: 有机太阳能电池, 热稳定性, 效率, 三元策略

As an emerging high-efficiency solar cell, organic solar cells (OSCs) have been developed rapidly in recent years. The power conversion efficiency (PCE) of OSCs has reached more than 19%, which is the dawn of commercial application. However, the stability of OSCs is not yet satisfied, especially high processing and operation temperature may be applied to the cells, which requires a high thermal stability of the cells. The ternary strategy, where a third component is introduced into the photoactive layer of donor-acceptor based binary OSCs, was found to be able to simultaneously improve device performance and stability by regulating the intermolecular interactions, showing a great potential for application. In this review, we firstly summarized the mechanisms involved in the thermal decay process of OSCs, including thermally induced morphology changes of the photoactive layer, interfacial aging/chemical reactions, and interdiffusion behavior between the layers. Following this, the research progress of the ternary strategies in improving thermal stability are highlighted, and the mechanism for the stabilization effect is reviewed. By the end, the perspective of the ternary strategies in OSCs is given, pointing out that the selection of the proper third component and the understanding on the mechanism of the stabilization effect are the key issues and challenges.

Key words: organic solar cell, thermal stability, efficiency, ternary strategy

引用此文

查汉, 房进, 闫翎鹏, 杨永珍, 马昌期. 有机太阳能电池热失效机制及三元共混提升其热稳定性研究进展[J]. 化学学报, 2023, 81(2): 131-145.

Han Zha, Jin Fang, Lingpeng Yan, Yongzhen Yang, Changqi Ma. Research Progress of Thermal Failure Mechanism and Ternary Blending to Improve Thermal Stability of Organic Solar Cells[J]. Acta Chimica Sinica, 2023, 81(2): 131-145.

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图/表 13

图1. T-OSCs的工作机制示意图: (a) 电荷转移; (b) 能量转移; (c) 平行模型; (d) 合金模型

Figure 1. Schematic diagram of the working mechanism of T-OSCs: (a) charge transfer; (b) energy transfer; (c) parallel model; (d) alloy model

图2. (a) 退火温度、时间与结晶的关系. (b) ITIC等温结晶的示意图. (c) Tcc、相分离和稳定性关系示意图

Figure 2. (a) Relationship between annealing temperature, time and crystallization. Reproduced with permission[49]. Copyright 2013, Royal Society of Chemistry. (b) Schematic illustrating isothermal crystallization of ITIC. Reproduced with permission[50]. Copyright 2019, ACS Publications. (c) Schematic diagram of the relationship between Tcc, phase separation and stability. Reproduced with permission[51]. Copyright 2019, Cell Press

图3. χ与小分子受体含量的相图关系

图4. (a) 在PEDOT:PSS基板上160 ℃热退火的三维形貌演变示意图

图5. 电极、传输层和活性层互相扩散示意图

图6. (a)光老化后热老化和热老化后光老化的JSC衰减. (b) PEI或PEIE与ITIC受体反应示意图. (c)在120 ℃下加热的PEDOT:PSS薄膜的电导率下降, PEDOT:PSS加热变化的三个阶段: (I) PSS链相互纠缠; (II) PEDOT和PSS链之间的离子键开始断裂; (III) PEDOT低聚物开始形成导电颗粒

Figure 6. (a) JSC decay diagram of photo-aging followed by thermal aging and thermal aging followed by photo-aging. Reproduced with permission[82]. Copyright 2019, Royal Society of Chemistry. (b) The schematic diagram of the reaction between PEI or PEIE and the ITIC acceptor. Reproduced with permission[40]. Copyright 2018, Royal Society of Chemistry. (c) Conductivity degradation of PEDOT:PSS films heated at 120 ℃, PEDOT:PSS heating changes in three stages: (I) PSS chains are entangled with each other; (II) ionic bonds between PEDOT and PSS chains start to break; (III) PEDOT oligomers start to form conductive particles. Reproduced with permission[85]. Copyright 2009, Elsevier

图7. (a, b) DFT计算优化的PM6和PBB1-Cl的堆积结构图. (c) 基于PM6:Y6-BO-4Cl的二元和优化三元OSCs在100 ℃下的热稳定性. (d, e) 二元OSCs和基于PBB1-Cl的三元共混膜的吸收光谱在100 ℃随加热时间的变化. (f) PM6:Y6-BO-4Cl、PM6:PBB1-Cl:Y6-BO-4Cl和PM6:PBB2-Cl:Y6-BO-4Cl共混材料加热过程中的DSC曲线

Figure 7. (a, b) The DFT calculation diagrams of the optimized stacking structures of PM6 and PBB1-Cl. (c) Thermal stability (100 ℃) of PM6:Y6-BO-4Cl based binary and optimized ternary OSCs. (d, e) The changes of binary OSCs and PBB1-Cl based ternary blend films absorption spectra with heating time at 100 ℃. (f) The DSC curves during the heating process of PM6:Y6-BO-4Cl, PM6:PBB1-Cl:Y6-BO-4Cl and PM6:PBB2-Cl:Y6-BO-4Cl blend materials. Reproduced with permission[89]. Copyright 2021, Royal Society of Chemistry

图8. (a) 未掺杂和掺杂1% (w) PZ1的PM6:BDTTT-2Cl共混物在150和110 ℃下的归一化光伏性能随退火时间的变化. (b) 未掺杂和掺杂PZ1薄膜在热应力作用下的AFM图像. (c) 在OOP方向和IP方向上相应共混物的一维GIWAXS曲线图. (d) PM6:Y6、PM6:Y6:PITIC-Ph共混膜在150 ℃下加热不同时间的器件性能变化. (e) 在150 ℃加热560 h后共混膜的OM和AFM图像. (f) 长期热退火后共混膜形貌示意图

Figure 8. (a) Normalized photovoltaic performance of the investigated PM6:BDTTT-2Cl blends without and with 1% (w) PZ1 as a function of annealing time at 150 ?℃ and 110 ?℃, respectively. (b) Surface topographic AFM images of the undoped and PZ1-doped films under thermal stress. (c) The one-dimensional GIWAXS line curves of the corresponding blends with respect to the OOP and IP directions. Reproduced with permission[33]. Copyright 2020, Springer Nature. (d) Thermal stressing (150 ℃) of PM6:Y6, PM6:Y6:PITIC-Ph blend films for various testing periods and performance of corresponding devices. (e) OM and AFM images of blend films after applying thermal stress at 150 ℃ for 560 h. (f) Cartoon representation of the blend morphology after long-term thermal annealing. Reproduced with permission[105]. Copyright 2021, Royal Society of Chemistry

图9. (a) PTB7、PTB7-th、PffBT4T-2OD、p-DTS(FBTTh2)2、PBDTTT-C-T、P3HT和BPO的分子结构. (b) 活性层中的给体、PC71BM, BPO和氢键示意图

Figure 9. (a) Molecular structures of PTB7, PTB7-th, PffBT4T-2OD, p-DTS(FBTTh2)2, PBDTTT-C-T, P3HT and BPO. (b) Schematic illustration of donor, PC71BM, BPO and hydrogen bond in active layer. Reproduced with permission[91]. Copyright 2016, Wiley-VCH

图10. (a~d) D1:D2:A型和(e~h) D:A1:A2型TOSCs中的(a, e)高效电荷转移, (b, f)高效电荷传输, (c, g)高效量子产率和(d, h)平衡电荷转移和传输的形貌模型示意图

Figure 10. Schematic diagrams of (a~d) D1:D2:A and (e~h) D:A1:A2 TOSCs in (a, e) efficient charge transfer, (b, f) effective charge transport, (c, g) efficient quantum yield and (d, h) balanced charge transfer and transport morphology models. Reproduced with permission[115]. Copyright 2020 Wiley-VCH

图11. (a) 富勒烯清除自由基机理示意图. (b) NFA及其主要反应位点的自氧化循环以及自由基猝灭位点

Figure 11. (a) Schematic diagram of the radical scavenging mechanism of fullerenes. Reproduced with permission[35]. Copyright 2021, ACS Publications. (b) Autoxidation cycle of NFA and its main reaction sites as well as the radical burst sites. Reproduced with permission[120]. Copyright 2019, Royal Society of Chemistry

图12. BZ4F-5, BZ4F-6和BZ4F-7分子的(a)端基π-π堆积距离与热扩散系数D的关系. (b)在薄膜中的声子转移和分子堆积示意图. PM6, Y7, N2200, PC71BM和ICBA的(c)原始薄膜的D值. (d)共混膜的D值. (e)器件的热衰减曲线

Figure 12. (a) Relationship between end-group π-π stacking distance and D for BZ4F-5, BZ4F-6 and BZ4F-7 molecules. (b) Schematic diagram of phonon transfer and molecular stacking in the films. Reproduced with permission[36]. Copyright 2021, Wiley-VCH. (c) D values of PM6, Y7, N2200, PC71BM and ICBA. (d) D values of the blend films. (e) Thermal decay curves of the four devices. Reproduced with permission[93]. Copyright 2022, AIP Publishing

图13. 三元策略提高器件热稳定性作用机制示意图

Figure 13. Diagram of the mechanism of ternary strategy to improve thermal stability of devices

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有机太阳能电池热失效机制及三元共混提升其热稳定性研究进展

Research Progress of Thermal Failure Mechanism and Ternary Blending to Improve Thermal Stability of Organic Solar Cells

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