Synthesis and thermal properties of two novel crystalline boron-aluminium chlorides

Acta Chimica Sinica ›› 1995, Vol. 53 ›› Issue (11): 1106-1111. Previous Articles Next Articles

Original Articles

两种新型氯化硼铝晶体的合成与热分解过程研究

于吉红;徐如人;徐柏庆

吉林大学化学系无机水热合成重点实验室;大连理工大学化学系

发布日期:1995-11-15

Synthesis and thermal properties of two novel crystalline boron-aluminium chlorides

YU JIHONG;XU RUREN;XU BAIQING

Published:1995-11-15

Abstract

Two novel crystalline boron-alluminium chloride B-C(1) and microporous boron-aluminium chloride BAC(10) with cationic framework, have been hydrothermally synthesized in the system B2O3-Al2O3-CaO-H2O at 200℃ and 160℃, respectively. Chemical analysis gives their product composition B-C(1):0.01B2O3:1.0Al2O3.0.4HCl.0.8H2O; BAC(10):0.5B2O3.1.0Al2O3.0.4HCl.3.0H2O. Their thermal properties are characterized by DTA-TG, TPDE-MS, XRD.

Key words: WATER, ALUMINIUM OXIDE, X-RAY DIFFRACTION ANALYSIS, MASS SPECTROGRAPHY, THERMAL STABILITY, CALCIUM OXIDE, DIFFERENTIAL THERMAL ANALYSIS, BORON OXIDE, THERMAL DECOMPOSITION

CLC Number:

O612

Cite this article

YU JIHONG;XU RUREN;XU BAIQING. Synthesis and thermal properties of two novel crystalline boron-aluminium chlorides[J]. Acta Chimica Sinica, 1995, 53(11): 1106-1111.

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两种新型氯化硼铝晶体的合成与热分解过程研究

Synthesis and thermal properties of two novel crystalline boron-aluminium chlorides

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