Synthesis and Characterization of Azacyclophanes Containing 1,3,5-Triazine

Chin. J. Org. Chem. ›› 2010, Vol. 30 ›› Issue (05): 745-748. Previous Articles Next Articles

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含均三嗪环氮杂环蕃合成与表征

吕国华, 花成文, 苟小锋, 刘艳凤

(西北大学化学与材料科学学院合成与天然功能分子化学教育部重点实验室西安 710069)

收稿日期:2009-09-08 修回日期:2009-11-25 发布日期:2009-12-17
通讯作者: 花成文 E-mail:huachengwen@126.com

Synthesis and Characterization of Azacyclophanes Containing 1,3,5-Triazine

Lü Guo-Hua , HUA Cheng-Wen, GOU Xiao-Feng, LIU Yan-Feng

(Key Laboratory of Synthetic and Natural Functional Molecule Chemistry, Ministry of Education, College of Chemistry & Materials Science, Northwest University, Xi an 710069)

Received:2009-09-08 Revised:2009-11-25 Published:2009-12-17

Abstract

Cyclophane with a cavity structure, has a great potential prospects. Some novel azacyclophanes were synthesized from cyanuric chloride, phenol, sodium methoxide, 1,6-hexane diamine and 4,4 -diaminodiphenyl methane by substitution, and their structures were characterized by ¹H NMR, IR, MALDI-TOF-MS techniques and elemental analysis. A large number of experiments have been carried out to explore the solvent, alkal and concentration to find out the best reaction conditions.

Key words: cyanuric chloride, cyclophane, synthesis, characterization

Cite this article

吕Guo-Hua , HUA Cheng-Wen, GOU Xiao-Feng, LIU Yan-Feng. Synthesis and Characterization of Azacyclophanes Containing 1,3,5-Triazine[J]. Chin. J. Org. Chem., 2010, 30(05): 745-748.

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含均三嗪环氮杂环蕃合成与表征

Synthesis and Characterization of Azacyclophanes Containing 1,3,5-Triazine

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