Studies of p-Hydroxy Pentiptycene Diazonium Salts and Their Replacement Reactions

Chin. J. Org. Chem. ›› 2009, Vol. 29 ›› Issue (11): 1816-1820. Previous Articles Next Articles

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对羟基五蝶烯重氮盐及其置换反应研究

谭广慧^a 王宇^a 王进军^b 金英学^*,a

(a哈尔滨师范大学化学化工学院哈尔滨 150025) (b烟台大学化学生物理工学院烟台 264005)

收稿日期:2009-03-14 修回日期:2009-05-27 发布日期:2009-06-30
通讯作者: 金英学 E-mail:yenghak@hrbnu.edu.cn

Studies of p-Hydroxy Pentiptycene Diazonium Salts and Their Replacement Reactions

Tan, Guanghui^a Wang, Yu^a Wang, Jinjun^b Jin, Yingxue^*,a

(^aCollege of Chemistry & Engineering, Harbin Normal University, Harbin 150025) (^b Science and Engineering College of Chemistry and Biology, Yantai University, Yantai 264005)

Received:2009-03-14 Revised:2009-05-27 Published:2009-06-30

Abstract

p-Aminopentiptycene phenol was formed by treating pentiptycene quinone through oxidation and hydrogenation. p-Pentiptycene phenol diazonium salts were synthesized by diazotization of p-amino- pentiptycene phenol with t-BuONO under acidity conditions. Their halides were obtained by Sandmeyer re-actions. The structures of all compounds were characterized by IR, FAB-MS, and NMR techniques.

Key words: pentiptycene, diazonium salt, Sandmeyer reaction, synthesis

Cite this article

TAN An-Hui, WANG Yu, WANG Jin-Jun, JIN Yang-Hua. Studies of p-Hydroxy Pentiptycene Diazonium Salts and Their Replacement Reactions[J]. Chin. J. Org. Chem., 2009, 29(11): 1816-1820.

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对羟基五蝶烯重氮盐及其置换反应研究

Studies of p-Hydroxy Pentiptycene Diazonium Salts and Their Replacement Reactions

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