Synthesis of β-Sulfinyl-N,N-di-n-butyl Propanamide

Chinese Journal of Organic Chemistry ›› 2004, Vol. 24 ›› Issue (1): 109-112. Previous Articles

β-亚磺酰基-N,N-二正丁基丙酰胺的合成研究

赵蓓^*, 陆澄容, 沈琪

苏州大学化学化工学院苏州 215006

收稿日期:2003-04-14 修回日期:2003-06-27 接受日期:2003-08-27 发布日期:2022-09-21
基金资助:
江苏省有机合成重点实验室开放基金(No. KJSO1019)资助项目.

Synthesis of β-Sulfinyl-N,N-di-n-butyl Propanamide

ZHAO Bei^*, LU Cheng-Rong, SHEN Qi

College of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215006

Received:2003-04-14 Revised:2003-06-27 Accepted:2003-08-27 Published:2022-09-21
Contact: *E-mail: orgsub@suda.edu.cn; Fax: 0512-65112371

Abstract

Six new compounds named β-sufinyl-N,N-di-n-butyl propanamides were synthesized by direct oxidation of β-alkylthio-N,N-di-n-butyl propanamides with hydrogen peroxide. These compounds were characterized by IR, ¹H NMR, MS and elemental analysis. Researches on extraction of trivalent rare earth ions with β-sulfinyl-N,N-di-n-butylpropanamides were performed under different conditions.

Key words: β-alkylthio-N,N-di-n-butyl propanamide, β-sulfinyl-N,N-di-n-butyl propanamide, oxidation, synthesis, extraction

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ZHAO Bei, LU Cheng-Rong, SHEN Qi. Synthesis of β-Sulfinyl-N,N-di-n-butyl Propanamide[J]. Chinese Journal of Organic Chemistry, 2004, 24(1): 109-112.

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β-亚磺酰基-N,N-二正丁基丙酰胺的合成研究

Synthesis of β-Sulfinyl-N,N-di-n-butyl Propanamide

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