Abstract：Nest-like Ag microcrystals were prepared by electrochemical methods. Synthetic parameters were elucidated, including deposition potential, temperature and concentration that can systematically control branching or faceting growth during electrodeposition process. SEM, XRD and surface enhanced Raman spectroscopy (SERS) were employed to characterize the structure and properties of nest-like Ag microcrystals. The nest-like Ag microcrystals show the enhanced SERS for Rhodamine 6G, and the Raman enhancement factor reaches 1.7×106.
范建凤, 赵晨醒, 范楼珍. 巢状微结构银粒子的制备、形成机理及表面增强拉曼光谱研究[J]. 化学学报, 2012, 70(03): 229-234.
Fan Jianfeng, Zhao Chenxing, Fan Louzhen. Preparation and Mechanism of Nest-like Ag Microcrystals and Their Surface Enhanced Raman Spectroscopic Studies. Acta Chimica Sinica, 2012, 70(03): 229-234.