Acta Chimica Sinica ›› 2021, Vol. 79 ›› Issue (4): 459-471.DOI: 10.6023/A20100494 Previous Articles Next Articles
Review
李旭飞a,b, 闫保有b, 黄维秋a,b,*(), 浮历沛b, 孙宪航b, 吕爱华b
投稿日期:
2020-10-27
发布日期:
2020-12-11
通讯作者:
黄维秋
作者简介:
李旭飞, 男, 常州大学材料科学与工程学院在读博士研究生, 目前在常州大学油气回收工程技术研究中心参与重点研发项目, 主要从事MOF及其复合材料的设计、制备及吸附分离应用. |
闫保有, 男, 常州大学石油工程学院在读硕士研究生, 目前在常州大学油气回收工程技术研究中心参与重点研发项目, 主要从事MOF材料的合成及其在有机废气治理中应用. |
黄维秋, 男, 常州大学石油工程学院教授, 博士生导师, 江苏省“油气回收基础理论及其应用”科技创新团队带头人, 江苏省“333工程”中青年科技领军人才, 江苏省有机废气资源化工程技术中心主任. 30多年来, 组建省级团队在国内率先并长期开展以“油气回收”为代表的有机废气污染控制及资源化的基础研究及技术开发取得丰富工作积累及系列创新成果, 并成功实现产业化. 目前主要研究方向: 油气回收基础理论及应用、石油储存工艺和新型纳米功能材料及其在有机废气治理中应用. |
浮历沛, 男, 博士, 江苏省高层次创新创业人才引进计划“科技副总”, 任教于常州大学石油工程学院. 近年来, 主持国家自然科学基金青年基金项目1项, 参与多项国家级项目研究, 发表论文多篇. 目前主要研究方向: 储运环保技术、新型功能材料开发及应用. |
孙宪航, 男, 博士, 任教于常州大学石油工程学院. 参与多项国家级项目研究, 发表论文多篇. 目前主要研究方向: 油气回收技术, 活性炭脱附研究. |
吕爱华, 女, 南京工业大学在读博士研究生, 任教于常州大学石油工程学院. 参与多项国家级项目研究, 发表论文多篇. 目前主要研究方向: 多孔介质传热传质及油气回收环保技术. |
基金资助:
Xufei Lia,b, Baoyou Yanb, Weiqiu Huanga,b,*(), Lipei Fub, Xianhang Sunb, Aihua Lvb
Received:
2020-10-27
Published:
2020-12-11
Contact:
Weiqiu Huang
About author:
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Xufei Li, Baoyou Yan, Weiqiu Huang, Lipei Fu, Xianhang Sun, Aihua Lv. Research Progress in Metal-Organic Framework and Its Composites for Separation of C2 Based on Sieving Multiple Effects[J]. Acta Chimica Sinica, 2021, 79(4): 459-471.
阴离子 | 键能△E/(kJ•mol–1) | 键能差/(kJ•mol–1) | |
---|---|---|---|
C2H2 | C2H4 | ||
B12H122– | –40.2 | –25.6 | 14.6 |
Cl– | –39.5 | –27.8 | 11.7 |
Br– | –37.4 | –30.4 | 7.0 |
SiF62– | –52.9 | –39.8 | 13.1 |
BF4– | –31.5 | –25.1 | 6.4 |
Tf2N– | –23.5 | –17.1 | 6.4 |
阴离子 | 键能△E/(kJ•mol–1) | 键能差/(kJ•mol–1) | |
---|---|---|---|
C2H2 | C2H4 | ||
B12H122– | –40.2 | –25.6 | 14.6 |
Cl– | –39.5 | –27.8 | 11.7 |
Br– | –37.4 | –30.4 | 7.0 |
SiF62– | –52.9 | –39.8 | 13.1 |
BF4– | –31.5 | –25.1 | 6.4 |
Tf2N– | –23.5 | –17.1 | 6.4 |
MOF | 材料孔径/ (nm×nm) | BET/ (m2•g–1) | C2H2吸附量/ (mmol•g–1) | C2H4吸附量/ (mmol•g–1) | 温度/ K | IAST选择性 (1∶99) | C2H4纯度/ % | 穿透时间b/ (min•g–1) | 参考文献 |
---|---|---|---|---|---|---|---|---|---|
M’MOF-3a | 0.34×0.48 | 110 | 1.90 | 0.40 | 295 | 5 | — | — | [ |
Mn(Ⅱ)-Mn(Ⅲ) | 0.55×0.40 | 362a | 3.20 | 0.24 | 283 | 16 | — | 18c | [ |
UTSA-100a | 0.43×0.43 | 970 | 4.27 | 1.66 | 296 | 11 | — | 17 | [ |
SIFSIX-3-Zn | 0.42×0.42 | 250 | 3.64 | 2.24 | 298 | 9 | 99.998 | 100 | [ |
SIFSIX-3-Ni | 0.42×0.42 | 368 | 3.30 | 1.75 | 298 | 5 | 99.998 | — | [ |
SIFSIX-2-Cu-i | 0.52×0.52 | 503 | 4.02 | 2.19 | 298 | 55 | 99.998 | 800 | [ |
SIFSIX-1-Cu | 0.80×0.80 | 1178 | 8.50 | 4.11 | 298 | 11 | 99.998 | 600 | [ |
UTSA-220 | 0.30×0.32 0.40×0.65 | 577 | 3.40 | 2.53 | 298 | 10 | 99.9999 | 125 | [ |
UTSA-200a | 0.34×0.34 | 612 | 3.65 | 0.63 | 298 | 6320 | 99.9999 | 1500 | [ |
ZU-32 | 0.35×0.35 | 467 | 3.97 | 2.19 | 298 | 67 | 99.999 | 800 | [ |
ZU-33 | 0.33×0.33 | 424 | 3.78 | 0.70 | 298 | 1100 | 99.9999 | 1600 | [ |
MOF | 材料孔径/ (nm×nm) | BET/ (m2•g–1) | C2H2吸附量/ (mmol•g–1) | C2H4吸附量/ (mmol•g–1) | 温度/ K | IAST选择性 (1∶99) | C2H4纯度/ % | 穿透时间b/ (min•g–1) | 参考文献 |
---|---|---|---|---|---|---|---|---|---|
M’MOF-3a | 0.34×0.48 | 110 | 1.90 | 0.40 | 295 | 5 | — | — | [ |
Mn(Ⅱ)-Mn(Ⅲ) | 0.55×0.40 | 362a | 3.20 | 0.24 | 283 | 16 | — | 18c | [ |
UTSA-100a | 0.43×0.43 | 970 | 4.27 | 1.66 | 296 | 11 | — | 17 | [ |
SIFSIX-3-Zn | 0.42×0.42 | 250 | 3.64 | 2.24 | 298 | 9 | 99.998 | 100 | [ |
SIFSIX-3-Ni | 0.42×0.42 | 368 | 3.30 | 1.75 | 298 | 5 | 99.998 | — | [ |
SIFSIX-2-Cu-i | 0.52×0.52 | 503 | 4.02 | 2.19 | 298 | 55 | 99.998 | 800 | [ |
SIFSIX-1-Cu | 0.80×0.80 | 1178 | 8.50 | 4.11 | 298 | 11 | 99.998 | 600 | [ |
UTSA-220 | 0.30×0.32 0.40×0.65 | 577 | 3.40 | 2.53 | 298 | 10 | 99.9999 | 125 | [ |
UTSA-200a | 0.34×0.34 | 612 | 3.65 | 0.63 | 298 | 6320 | 99.9999 | 1500 | [ |
ZU-32 | 0.35×0.35 | 467 | 3.97 | 2.19 | 298 | 67 | 99.999 | 800 | [ |
ZU-33 | 0.33×0.33 | 424 | 3.78 | 0.70 | 298 | 1100 | 99.9999 | 1600 | [ |
MOF | 材料孔径/ (nm×nm) | BET/ (m2•g–1) | C2H2吸附量/ (mmol•g–1) | C2H4吸附量/ (mmol•g–1) | 温度/ K | IAST选择性 (1∶99) | C2H4纯度/% | 穿透时间/ (min•g–1) | 参考文献 |
---|---|---|---|---|---|---|---|---|---|
ELM-11 | — | — | 3.5 | 0.06 | 298 | 60a | — | 9a | [ |
ELM-13 | — | — | 3.0 | 0.18 | 298 | 10000a | — | 6 | [ |
NTU-65 | 0.26×0.34 0.52×0.63 | 680 | 3.36 | 0.05 | 298 | — | 99.95 | 85 | [ |
UTSA-300a | 0.35×0.39 | 311 | 3.08 | 0.04 | 298 | 75b | 99.9 | 12b | [ |
NCU-100a | 0.36×0.43 | 358 | 4.57 | 0.32 | 298 | 7291 | 99.9995 | 167 | [ |
MOF | 材料孔径/ (nm×nm) | BET/ (m2•g–1) | C2H2吸附量/ (mmol•g–1) | C2H4吸附量/ (mmol•g–1) | 温度/ K | IAST选择性 (1∶99) | C2H4纯度/% | 穿透时间/ (min•g–1) | 参考文献 |
---|---|---|---|---|---|---|---|---|---|
ELM-11 | — | — | 3.5 | 0.06 | 298 | 60a | — | 9a | [ |
ELM-13 | — | — | 3.0 | 0.18 | 298 | 10000a | — | 6 | [ |
NTU-65 | 0.26×0.34 0.52×0.63 | 680 | 3.36 | 0.05 | 298 | — | 99.95 | 85 | [ |
UTSA-300a | 0.35×0.39 | 311 | 3.08 | 0.04 | 298 | 75b | 99.9 | 12b | [ |
NCU-100a | 0.36×0.43 | 358 | 4.57 | 0.32 | 298 | 7291 | 99.9995 | 167 | [ |
分离方式 | MOF | 材料孔径/ (nm×nm) | BET/ (m2•g–1) | C2H4吸附量/ (mmol•g–1) | C2H6吸附量/ (mmol•g–1) | 温度/ K | IAST选择性 (50∶50) | C2H4纯度/% | 穿透时间/ (min•g–1) | 参考 文献 |
---|---|---|---|---|---|---|---|---|---|---|
C2H4选择性吸附筛分 | Ni-gallate | 0.347×0.485 | 424 | 2.00 | 0.28 | 298 | 16.8 | — | 83 | [ |
Mg-gallate | 0.356×0.484 | 559 | 3.00 | 0.26 | 298 | 37.3 | — | 162 | [ | |
Co-gallate | 0.369×0.495 | 475 | 3.37 | 0.31 | 298 | 52.0 | — | 138 | [ | |
UTSA-280 | 0.380×0.380 0.320×0.450 | 331 | 2.50 | 0.10 | 298 | >104 | — | 30 | [ | |
UTSA-280-M1 | — | — | 2.20 | 0.05 | 298 | 1100 | — | 35 | [ | |
UTSA-280-M2 | — | — | 2.83 | 0.05 | 298 | 1200 | — | 50 | [ | |
C2H6选择性吸附筛分 | Fe2(O2)(dobdc) | — | 1073 | 2.63 | 3.32 | 298 | 4.4 | 99.99 | 15 | [ |
MUF-15 | 0.850×0.350 0.700×0.380 0.320×0.120 | 1130 | 4.15 | 4.69 | 293 | 2.0 | 99.95 | 20 | [ | |
MAF-49 | 0.330×0.300 | — | 1.65 | 1.70 | 316 | 2.7 | 99.986 | 170 | [ | |
NJU-2 | 0.420×0.420 0.720×0.720 0.920×0.920 0.370×0.370 | 1219 | 3.62 | 4.19 | 298 | 1.6 | 99.99 | 100 | [ |
分离方式 | MOF | 材料孔径/ (nm×nm) | BET/ (m2•g–1) | C2H4吸附量/ (mmol•g–1) | C2H6吸附量/ (mmol•g–1) | 温度/ K | IAST选择性 (50∶50) | C2H4纯度/% | 穿透时间/ (min•g–1) | 参考 文献 |
---|---|---|---|---|---|---|---|---|---|---|
C2H4选择性吸附筛分 | Ni-gallate | 0.347×0.485 | 424 | 2.00 | 0.28 | 298 | 16.8 | — | 83 | [ |
Mg-gallate | 0.356×0.484 | 559 | 3.00 | 0.26 | 298 | 37.3 | — | 162 | [ | |
Co-gallate | 0.369×0.495 | 475 | 3.37 | 0.31 | 298 | 52.0 | — | 138 | [ | |
UTSA-280 | 0.380×0.380 0.320×0.450 | 331 | 2.50 | 0.10 | 298 | >104 | — | 30 | [ | |
UTSA-280-M1 | — | — | 2.20 | 0.05 | 298 | 1100 | — | 35 | [ | |
UTSA-280-M2 | — | — | 2.83 | 0.05 | 298 | 1200 | — | 50 | [ | |
C2H6选择性吸附筛分 | Fe2(O2)(dobdc) | — | 1073 | 2.63 | 3.32 | 298 | 4.4 | 99.99 | 15 | [ |
MUF-15 | 0.850×0.350 0.700×0.380 0.320×0.120 | 1130 | 4.15 | 4.69 | 293 | 2.0 | 99.95 | 20 | [ | |
MAF-49 | 0.330×0.300 | — | 1.65 | 1.70 | 316 | 2.7 | 99.986 | 170 | [ | |
NJU-2 | 0.420×0.420 0.720×0.720 0.920×0.920 0.370×0.370 | 1219 | 3.62 | 4.19 | 298 | 1.6 | 99.99 | 100 | [ |
ZIF | 组成 | BET/(m2•g–1) | 孔径/nm | 笼径/nm | 参考文献 |
---|---|---|---|---|---|
ZIF-65 | Co(nIm)2 | 760 | 3.4 | 10.4 | [ |
ZIF-67 | Co(mIm)2 | 1280 | 3.4 | 11.6 | [ |
ZIF-71 | Zn(dcIm)2 | 827 | 4.2 | 16.5 | [ |
ZIF-8 | Zn(mIm)2 | 1947 | 3.4 | 11.6 | [ |
ZIF-90 | Zn(Ica)2 | 1270 | 3.5 | 11.2 | [ |
ZIF-95 | Zn(cbIm)2 | 1050 | 3.7 | 24 | [ |
ZIF-100 | Zn20(cbIm)39(OH) | 595 | 3.4 | 35.6 | [ |
ZIF | 组成 | BET/(m2•g–1) | 孔径/nm | 笼径/nm | 参考文献 |
---|---|---|---|---|---|
ZIF-65 | Co(nIm)2 | 760 | 3.4 | 10.4 | [ |
ZIF-67 | Co(mIm)2 | 1280 | 3.4 | 11.6 | [ |
ZIF-71 | Zn(dcIm)2 | 827 | 4.2 | 16.5 | [ |
ZIF-8 | Zn(mIm)2 | 1947 | 3.4 | 11.6 | [ |
ZIF-90 | Zn(Ica)2 | 1270 | 3.5 | 11.2 | [ |
ZIF-95 | Zn(cbIm)2 | 1050 | 3.7 | 24 | [ |
ZIF-100 | Zn20(cbIm)39(OH) | 595 | 3.4 | 35.6 | [ |
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