有机化学 ›› 2003, Vol. 23 ›› Issue (10): 1152-1154. 上一篇    下一篇

研究论文

微波辐射下2-氨基苯并[h]喹唑啉衍生物的合成

王香善;史达清;王苏惠;屠树江   

  1. 徐州师范大学化学系
  • 发布日期:2003-10-25

Synthesis of 2-Amino-benzo[h]quinazoline Derivatives under Microwave Irradiation

Wang Xiangshan;Shi Daqing;Wang Suhui;Tu Shujiang   

  1. Department of Chemistry, Xuzhou Normal University
  • Published:2003-10-25

2-芳亚甲基-3,4-二氢-2H-1(2H)-萘酮和碳酸胍在以乙二醇为溶剂、微波辐 射下反应,生成一系列新的2-氨基-4-芳基-5,6-二氢化苯并[h]喹啉衍生物,产物 的结构通过单晶X射线衍射分析确证。

关键词: 微波辐射, 喹唑啉 P, 萘酮 P, 胍, 乙二醇, X射线衍射分析

A series of new 2-amino-4-aryl-5,6-dihydro-benzo[h] quinazoline derivatives have been synthesized by the reaction of 2-arylmethylidene- 3,4-dihydro-1 (2H)-naphthalenone with guanidine carbonate in ethyleneglycol under microwave irradiation. The structure of the product was confirmed by X-ray analysis.

Key words: MICROWAVE RADIATION;QUINAZOLINE P;NAPHTHALENONE P;GUANIDINES, ETHANEDIOL;XRD

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