Synthesis and Characterization of Novel Schiff Base Macrocyclic Compounds of 1,3,5-Triazine

doi:10.6023/cjoc1110312

Chin. J. Org. Chem. ›› 2012, Vol. 32 ›› Issue (05): 939-942.DOI: 10.6023/cjoc1110312 Previous Articles Next Articles

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新型三嗪类席夫碱大环化合物的合成与表征

李小安, 花成文, 苟小锋, 赵军龙, 陈邦

西北大学化学与材料科学学院合成与天然功能分子化学教育部重点实验室西安 710069

收稿日期:2011-10-31 修回日期:2011-12-12 发布日期:2012-01-11
通讯作者: 花成文 E-mail:huachengwen@163.com

Synthesis and Characterization of Novel Schiff Base Macrocyclic Compounds of 1,3,5-Triazine

Li Xiaoan, Hua Chengwen, Gou Xiaofeng, Zhao Junlong, Chen Bang

Key Laboratory of Synthetic and Natural Functional Molecule Chemistry Ministry of Education,College of Chemistry and Materials Science, Northwest University, Xi'an 710069

Received:2011-10-31 Revised:2011-12-12 Published:2012-01-11

Several novel Schiff base macrocyclic compounds of 1,3,5-triazine were synthesized from cyanuric chloride, diethylamine, vanillin, o-phenylenediamine, p-phenylenediamine, benzidine, 4,4'-diamino-ether, 4,4'-diamino-diphenyl methane by substitution and cyclization, and their structures were characterized by ¹H NMR, IR, ESI/MS techniques and elemental analysis. The studies on the UV-Vis absorption spectroscopies show that Schiff base 3b has a selective recognition for Cu²⁺, and 3a, 3c for Fe³⁺.

Key words: cyanuric chloride, Schiff base, macrocyclic compound, synthesis, characterization

Cite this article

Li Xiaoan, Hua Chengwen, Gou Xiaofeng, Zhao Junlong, Chen Bang. Synthesis and Characterization of Novel Schiff Base Macrocyclic Compounds of 1,3,5-Triazine[J]. Chin. J. Org. Chem., 2012, 32(05): 939-942.

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新型三嗪类席夫碱大环化合物的合成与表征

Synthesis and Characterization of Novel Schiff Base Macrocyclic Compounds of 1,3,5-Triazine

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