有机化学 ›› 1996, Vol. 16 ›› Issue (3): 242-245. 上一篇    下一篇

研究论文

微波辐射下的芳基甲酰氨基硫脲的合成

史海健;王忠义;史好新;张自义   

  1. 安徽师范大学化学系;兰州大学化学系
  • 发布日期:1996-06-25

Synthesis of aroylthiosemicarbazides under microwave irradiation

SHI HAIJIAN;WANG ZHONGYI;SHI HAOXIN;ZHANG ZIYI   

  • Published:1996-06-25

本文报道了以水为介质, 在微波辐射下的芳基甲酰氨基硫脲的合成。该法反应快, 产率高。

关键词: 芳基甲酰肼, 红外分光光度法, 质子磁共振谱法, 芳基甲酰氨基硫脲, 有机合成, 微波辐射

This paper reported the synthesis of aroylthiosemicarbazides under the microwave irradiation. Compared with the conventional method, the reaction time was dramatically reduced and good yield was obtained.

Key words: PROTON MAGNETIC RESONANCE SPECTROMETRY, ORGANIC SYNTHESIS, MICROWAVE RADIATION, INFRARED SPECTROPHOTOMETRY

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